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GC/MS analysis results for sample AD22582, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087269
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Heptacosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.53 1.14 ug/1 138906 Perylene-dl2 37.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91

? 2 Heneicosane 296 C21H44 000629-94-7 90 3 Eicosane 282 C20H42 000112-95-8 89 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 87 Abundance Scan 3321 (35.531 min): 22582.D (-) m/z SYTOO 100.00% 57

85 5000 4

JJU-TtM 267283 I'' " i'''' I'''' I'''' I''" I'''' I :^.2O 35.40 35.60 35.80 m/z TIToO 7O73Y% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane 57

5000 85 '3'5'20' '3'5'40' '3'5.60' '35.8'0' m/z 43 :05 66745% 196 281224 324 380 TTTTTTTYTT'TTj'hmYrTYT^^ '' I " " I" " I " " I ‘" i" " I " " I'' " I" " I " " I " n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane 57

85 35.20 35,40 35,60 35.80 5000 m/z85.05 53.76%

Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #72323: Eicosane 5(7 :^.2O 35.40 35.60 35.80 m/z 55.00 24.44% 5000 85

,j.,, 'i.VjL/,........... .......... 3’5'40 s's'eo' '35.80' TlZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380

22582.D NP091101.M Wed Oct 03 12:09:23 2001 Page 12

NYC-WTC_000087269

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NYC-WTC_000087269Source: NYC Law Department, mirrored locally

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