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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial; 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Tetratetracontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.40 0.74 ug/1 89450 Perylene-dl2 37.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Pentatriacontane 493 C35H72 000630-07-9 91 4 Dotriacontane 451 C32H66 000544-85-4 91 <\bundance Scan 3416 (36.403 min): 22582.D (-) in/z SYTOO 100.00% 7

5000 85

Jipi41 36,00 36,20 36,40 36,60 36,80 183 239 281 355 m/z 71.05 66.51% ■nZz-> ^bundance 50 100 150 200 250 300 350 400 #61068: Tetratetracontane 450 500 550 600 (1 57

5000 85 36,00 36,20 36,40 36,60 36,80 m/z 43.05 63.70%

Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74635: Hexatriacontane 57

36.00 36.20 36.40 36,60 36,80 5000 85 m/z 85.05 45.69%

■nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #58743: Pentatriacontane T 57 36,00 36,20 36,40 36,60 36,80 24.21%

5000 85

^^^,14^169197225 T ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 600 36,00 36,20 36,40 36,60 36,80

22582.D NP091101.M Wed Oct 03 12:09:25 2001 Page 13

NYC-WTC_000087270

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NYC-WTC_000087270Source: NYC Law Department, mirrored locally

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