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GC/MS analysis results for sample AD22582, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087268
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *****************************************J(r*************************** Peak Number 11 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.64 1.07 ug/1 147673 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Nonadecane 268 C19H40 000629-92-5 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 3224 (34.641 min): 22582.D (-) m/z SYTOO 100.00% 71 43

5000 85

34.40 34.60 34.80 35.00 il, ,l, ‘•5® 169183197 225 240 256 281 m/z 71.00 70.90% ttZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 5000 34.40 34.60 34.80 35.00 99 m/zi 43 ; 05 64757% 268 296 I ' I ‘ ’ I ' ' • ' f ' I I ' ‘ ' I I ' ' ' ' I ' ' ' ' I ' n/z-> 40 60 80 log 120 140 160 180 200 220 240 260 280 300 Abundance 57

71 #71949: Nonadecane K I * ' 34.40 34.60 34.80 35.00 5000 m7z 85.00 49.42% 85

99 J 141 155169 183 224 268 I I ' ' " ' I ' ' ' ' r ' ' ' 'i I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 57 34.40 34.60 34.80 35.00 .... 71 5000 85

99 J 141 155169 210 240 ' I'''' I' 'I’'< 'I''• ' f''''I''''I I'' ' ' I ' ' ' ' I' y-TT-r-r-j- nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 34.40 34.60 34.80 35.00

22582.D NP091101.M Wed Oct 03 12:09:20 2001 Page 11

NYC-WTC_000087268

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NYC-WTC_000087268Source: NYC Law Department, mirrored locally

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