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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088419
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D Vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heneicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.73 3.97 ug/1 419819 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91, 2 Octadecane 254 C18H38 000593-45-3 91 3 Nonadecane 268 C19H40 000629-92-5 91 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 Abundance Scan 3017 (32.735 min): 23318.D (-) m/z 57.00 100.00% 57

85 5000

4 r-r-p-r-n-p ■ ' I I ' ' u 32.40 32.60 32.80 33.00 352 m/z 71710 69.81% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57

5000 85 V ' 'I 32.40 32.60 32.80 33.00 m/z 43.05 63.67% I 113 4...

■nZ2-> '' I'j UJX v X w r '' ‘ I' ’ ’' I''' I'''' I' 'I 268 296 I " ' • I ' "7 I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I " " I........... p-rrrp-rrrf

Abundance #71561: Octadecane 57-

32.40 32.60 32.80 33.00 85 5000 m/z S^ToT 50.58%

I I 113 141 224 254 111'' I " ' 111' " I' " ' I'''' I'' " I' " ' I " '' I' ’ " I''" I " '' I n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #71949: Nonadecane I 57 32.40 32.60 32.80 33.00 m/z 41.05 24.84% 5000 85

J T , 141 169 268 224 I ■'" I" ■ 11'"' r ’I "I ■1'''' I I'''' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23318.D NP091101.M Mon Oct 15 09:46:03 2001 Page 11

NYC-WTC_000088419

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NYC-WTC_000088419Source: NYC Law Department, mirrored locally

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