GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM \1\DATA\DEC0401\28692.D Vial: 19 Acq On 5 Dec 2001 5:56 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Hexatriacontane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.66 0.90 ug/1 159838 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 (91 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 3 Docosane 310 C22H46 000629-97-0 90 4 Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 2899 (31.659 min): 28692.D (-) m/z 57.00 100.00% 57 43 71 5000 85

T T I TT I I f I | I !‘ 11 ' | 99 31.40 31.60 31.80 32.00

miz-> 40 ‘II4 113127 141 155 169 60 80 207 TTT—TrTr T’’T I | I I I I | I I I > | ! I ! ! | ! ! ! I | I I I I | 100 120 140 160 180 200 220 240 260 280 300 > I | I I > > m/z 43.05 67.46% Abundance #74636: Hexatriacontane 43 57

71 5000 Tnumr 85 31.40 31.60 31.80 32.00 m/z71.00 66.66% li 39 113 127141 155169183197211 ■ ■ i ■' ■11'' TTTTmutnpmi, 1 r M ' r ■ ■ ■ i''1 ■ i'1 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- 57 71 — ) V 1TPPm U 31.40 31.60 31.80 32.00 5000 85 m/z 85.00 45.00%

mlz—> 40 ■ ■ ।11 M 2113127141155 60 TH 80 183 211 268 T’’’1—0u10’Cmuuur 100 120 140 160 180 200 220 240 260 280 300 296

Abundance 57 #44318: Docosane P 31.40 31.60 31.80 32.00 I ' ' ' ' I ‘ '

71 m/z 41.05 26.24% 85 5000

99

•' l1 ' ‘ 1 i ‘ r LL ] 113127141155 169 266 310 TTTTTer JV..... m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00

28692.D GCMS1126.M Thu Dec 06 12:39:36 2001 Page 6

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