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GCMS analysis comments for sample AD28691, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.

NYC-WTC_000035052–000035071

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035068
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28691.D Vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.53 1.09 ug/1 247833 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94) 2 Pentacosane 352 C25H52 000629-99-2 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Nonacosane 408 C29H60 000630-03-5 91 Abundance Scan 3212 (34.532 min): 28691 .D (-) m/z 56.95 100.00% 57 43 71

5000 85

TTTTmTTrr TT—BTT A111127141155169183197211 256 281 TTTuT -j-nr 34.20 34.40 34.60 34.80 m/z71.00 70.27% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

71 5000 TTRmu 4. । TTTTT Tr rr । 85 34.20 34.40 34.60 34.80 m/ z 43.00 67.34% . 1113127141155169183197211 . ........ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73718: Pentacosane 43 57 "FFTTPrrmfr । TUT TTTTT 71 34 20 34.40 34.60 34.80 5000 m/z 85.05 45.25% 85

QQ 44-

'1111 1 J 11127141155169183197211225 ........ ............ ...... mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002: Heneicosane, 11-(1-ethylpropyl)- TTTTTTpfuu, 43 57 34.20 34.40 34.60 34.80 m/z 55.0.0 26.71% 71 5000 85

m/z—> P................ 183197211225295 । । । . 1 J rii . । । 338 TTItrtIITTn . । t . । ‘T‘‘‘tII‘TT p m t । t t m । > । । । । rii > । ‘TT i J rn . । 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 tt।t। TT • I ‘ ' ''l1 M 1 I 34.20 34.40 34.60 34.80

28691.D GCMS1126.M Thu Dec 06 13:26:53 2001 Page 11

NYC-WTC_000035068

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NYC-WTC_000035068Source: NYC Law Department, mirrored locally

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