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GCMS analysis log for sample AD30696, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

NYC-WTC_000018123–000018141

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018136
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC3 101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heptadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

35.41 1.63 ug/1 229449 Perylene-d12 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 93 2 Triacontane 422 C30H62 000638-68-6 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance ’ Scan 3308 (35.410 mln): 30696.D (-) m/z 57.00 1 00.00% 57

5000 85 — mne R ' Lak.,441174141.169-20021RR 35.00 35.20 35.40 35.60 35.80 m/z 43.05 78.15% miz-> 40 60 80 100120140160180 200220240 260280 300 320 340360 380 400 420 Abundance #71194: Heptadecane 57

5000 i • • • ■ i T T 85 35.00 35.20 35.40 35.60 35.80 m/z 71. 10 62.03% . If3 , 141 169 212 240 TmrrrprT_ummu]pmmmnmpnmuemmn1mnm “PamgT m/z-> 40 60 80 100120140160180200 220240260280300320340360380400420 Abundance #55461: Triacontane 43 : TfR : 71 35.00 35.20 35.40 35.60 35.80 5000 m/z 85.05 44.82%

199 127 239 267 379 422 Wpgae T10uumu—uem00nT]mT m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73543: Tetracosane —10—T 57 35.00 35.20 35.40 35.60 35.80 m/z 41.00 29.33% 5000- 85

। | 113 , 155 183 294 338 mupnepr —rm1911191mm290—0—20000—B2202ppa miz-> 40 60 80 100120140160180200220240260280300320340360380400420 35.00 35.20 35.40 35.60 35.80

30696.D GCMS1126.M Wed Jan 23 08:37:02 2002 Page 7

NYC-WTC_000018136

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NYC-WTC_000018136Source: NYC Law Department, mirrored locally

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