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GCMS results log, sample AD26833, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.

NYC-WTC_000032286–000032307

Folder label: “GCMS X 11/8/01 A 12/7/01

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On : 7 Dec 2001 4:14 pm Operator: GALOS Sample : gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Heptadecane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

29.70 1.19 ng/uL 394507 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Q 1 Heptadecane 240 C17H36 000629-78-7 90 2 Eicosane 282 C20H42 000112-95-8 90 3 Nonadecane 268 C19H40 000629-92-5 86 4 10-Methylnonadecane 282 C20H42 _______ 000000-00-0 86 'Abundance Scan 2711 (29.703 min): 26833.D (-) m/z 57:10 100.00% ■ 57 43 71 5000 85 .............................................. ............. 1 1 — 99 29.40 29.60 29.80 30.00 i m/z-> .h 40 60 ++ 80 .1 113 127 141 155 TIITmTTmPTTTTPTTTT 100 120 140 160 180 200 220 240 260 280 m/z " 66.64% Abundance #71191: Heptadecane 43 57 71 5000- 85 29.40 29.60 29.80 30.00 m/ Z 71.05 62.40% - 99 113 127 141.............240...... I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane I 43 57

29.40 29.60 29.80 30.00 71 5000 m/z 85.05 39.97% 85

- ' .! 99 113 127 141 282 I ' ' i ' ■ i'' ■ ■ । ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #37469: Nonadecane A 43 57 71 29.40 29.60 29.80 30.00 m/z 41.10 28.82% 85 5000-

99 ■ ■ i ■ ' Il jiL H3 127 II 1111 * I 1 ' ’ 1 1 1 - 183 197 268 ’m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 29.40 29.60 29.80 30.00

26833.D NP112701.M Tue Dec 11 14:46:36 2001 Page 4

NYC-WTC_000032297

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NYC-WTC_000032297Source: NYC Law Department, mirrored locally

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