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GCMS results log, sample AD26833, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.

NYC-WTC_000032286–000032307

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032298
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1-Hexacosanol Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

29.83 0.59 ng/uL 194492 Chrysene-dl2 33.19 /

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1-Hexacosanol 382 C26H540 000506-52-5 47 2 1 -Hexadecanol 242 C16H340 036653-82-4 43 3 1 -Octadecanol 270 C18H380 000112-92-5 43 4 Nonadecanol 284 C19H40O 052783-43-4 37 Abundance Scan 2725 (29.832 min): 26833.D (-) m/z 143.05 100.00% 43

5000 61 83

AL > । i । 29.40 29.60 29.80 30.00 30.20 . । .

m/z-> 20 i'''1 P 40 160 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i •' " i'' ■ ■ r ■ " i ’ ■ ‘11 I •u 11 ■ ■' ■ i' ’ "I m/z 55.10 49.18% Abundance #52385: 1-Hexacosanol 43

5000- 83 29.40 29.60 29.80 30.00 30.20 m/z 61.00 46.76%

m/z-> i ■ ■ ■ ■ i' 20 40 60 UA 111

111" 11'"11 111111" ’' I' ' " I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 336 TTTTTT T’’].... 11. < 364

Abundance #71247: 1-Hexadecanol i 43 Tr 29.40 29.60 29.80 30.00 30.20 5000 83 m/ z 83.05 42.75% 27 . 111 196 224 । । ■. ■ ■ । ■ i ■ > >»।1 • TT I,,.. 1... 11111 > I 11 ‘1111 ’'11'' *' I m/z-> Abundance 20 40

43 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #72026: 1-Octadecanol AAA 29.40 29.60 29.80 30.00 30.20 m/z 69.10 40.96% 5000 - 83

i 27

m/z-> r ■ ■ ■ i ■ " 1 r 20 40 60 LUX 1 • * > H 1''' TTTTTT 224 252 ■ |" " 1" * ■ I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 l1 “ ’ I " 1' I'' •' I ’' • • I TIT 29.40 29.60 29.80 30.00 30.20

26833.D NP112701.M Tue Dec 11 14:46:38 2001 Page 5

NYC-WTC_000032298

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NYC-WTC_000032298Source: NYC Law Department, mirrored locally

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