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GCMS analysis results for sample AD28105, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28105 conducted on January 2, 2002.

NYC-WTC_000034642–000034652

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28105.D Vial: 12 Acq On : 22 Dec 2001 3:56 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Hexacosanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.73 0.55 ng/uL 138252 Chrysene-dl2 33.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexacosanol 382 C26H540 000506-52-5 43 2 Nonadecanol 284 C19H40O 052783-43-4 43 3 l-Tetracos :ol 354 C24H50O 000506-51-4 43 4 1-Eicosa] 1 298 C20H42O 000629-96-9 43 Abundance Scan 2714 (29.732 min): 28105.D (-) m/z 43.10 100.00% 43

5000 81 83

miz-> 20 | I I l ip l ITf! 111.. 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 29.40 29.60 29.80 30.00 ' m/z 55.10 45.31% Abundance #52385: 1-Hexacosanol 43

5000 83 29.40 29.60 29.80 30.00

6; 111 m/ z 57.10 42.34% I, , 336 364 । • ■ • ■ । ■ $‘ m/z- > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #40237: Nonadecanol 43 ......... /.... - 29.40 29.60 29.80 30.00 5000 83 m/z 61.1.0 41.84% 27 : 111 266 T"TTTTT‘TTT‘‘III‘IIIT TWTICIIIu TUTT TT TT , , TTTTT , rrTpHT-rp-H-rp-rr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49775:1-Tetracosanol ..................................................... 43 29.40 29'60 29.80 30.00 ' m/ z 83.15 39.52% 5000 83

6, || | | HI ,_________________________ 308 336 i r..।r..r,..i।।।।।।11..i. I' •' • I ” miz->20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ... .... 4......... 29.40 29.60 29.80 30.00

28105.D NP112701.M Fri Dec 28 09:55:09 2001 Page 2

NYC-WTC_000034651

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NYC-WTC_000034651Source: NYC Law Department, mirrored locally

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