GCMS analysis results for sample AD26626, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 Hexacosane Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

34.67 0.56 ng/uL 125742 Chrysene-dl2 33 .18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

366 C26H54 0 0 0 6 3 0 - 01-3 83- 1 Hexacosane 2 Eicosane 282 C20H42 000112-95-8 83 3 Heptadecane 240 C17H36 000629-78-7 78 4 Eicosane 282 C20H42 000112-95-8 64 Abundance Scan 3253 (34.669 min): 26626.D (-) m/ z 57.10 100.00% i 57 |

5000- 85 4 -i । । TTPI 1 TIT । । 1 34.40 34.60 34.80 35.00 TTr J 1 1113 ' । ■1 •1' ■ ” l ।i■irpii।। i । ! ।■ ■ ■■ । m/ Z 73.90% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73942: Hexacosane 57

5000 85 34.40 34.60 34.80 35.00 m/z 43. 0 68.11% 42 ■ ■ ।1 J V 1113....... 11 ” 1111' ’' 1111' 1 197 225 253 r 11 ‘ i ‘1" i 281 338 366 • I'1'' I ’''' 111'' I'' • ’1111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72323: Eicosane 57 MM— 34.40 34.60 34.80 35.00 5000 m/z 85.05 40.98% 85

42 113 141 282 I TTI’ i • ■ " r ' ■' i i1 • • ’ i * ’ • • i ■ •1' i11 •' i ′′′′′′′ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ■Abundance #71191: Heptadecane i ' ' ■ ' i ' ' I 57 34.40 34.60 34.80 35.00 m/z 41.10 27.82% 5000 85 ..... ........................ .......

j 113 . 141 |.ii.fit.>|, • r 11n। , । > < > 11 240 r ''' i''' • i1''' r ■ ■ ■ i ■' ‘' i I 1 “ 1 1 1 ' ’ 11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 34.40 34.60 34.80 35.00

26626.D NP112701.M Fri Dec 07 14:50:34 2001 Page 19

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