GCMS results log, sample AD27009, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Eicosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

32.79 2.04 ng/uL 907033 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 (9 2 Pentacosane 352 C25H52 000629-99-2 90 3 Eicosane, 10-methyl- 296 C21H44 054833-23-7 86 4 Heptadecane 240 C17H36 000629-78-7 86 Abundance Scan 3048 (32.791 min): 27009. D (-) m/ z 57.10 100.00% 57 43

5000 85 ------------

m/z-> 40 T A1 60 99 113 141155 182197 TTITTT -p-m-f I •’'‘I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00 33.20 m/ z 43.10 72.01% Abundance #72323: Eicosane 57

5000 85 32.40 32.60 32.80 33.00 33.20 m/z 71.05 61.47% 42 __ 2. T‘‘ M > .l1 ‘‘113127 "I1"TTTT l , "I1"11 ‘T""ITTTT‘TT 282 i । । । i t । i ■ TTT r TTITUTTTT I ’''' I ‘' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #49559: Pentacosane 4.3 -......... —PP T—PTTTT 71 32.40 32.60 32.80 33.00 33.20 5000 85 m/ Z 85.05 40.48%

113127 197 225239 267 325 352 0 TI1T TTT TT >i(..<11।।t । ।. 11 11 '1 11'1 1 ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42197: Eicosane, 10-methyl- ...... A 57 32.40 32.60 32.80 33.00 33.20 m/ Z 41.10 28.87% 5000- 85

42 I ■ ■ i'1 J 1 1 T’TTITETTTT 154169 | I! I ( | It !-f| 268 296 11'11 i11'' i1 r •••i•••‘i ----- • • I > • miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00 33.20

27009.D NP112701.M Tue Dec 11 14:59:37 2001 Page 8

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