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GCMS results log, sample AD27009, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27009 completed on December 11, 2001.

NYC-WTC_000032534–000032552

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heptadecane, 2,6,10 ,.15-tetrame Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.80 2.28 ng/uL 1012680 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 2 Heptadecane 3 Nonadecane 240 C17H36 268 C19H40 054833-48-6 000629-78-7 000629-92-5 86 00 4 Dodecane, 1-iodo-___________________ 296 C12H25I 004292-19-7 86 Abundance Scan 2940 (31.801 min): 27009.D (-) m/z 57.10 100.00% 57 43 71 5000 85 I ‘ - 1 1 I ' ' 1 i11 ' 11 11 1 1 - 99 113 31.40 31.60 31.80 32.00 32.20 +4 1 l — 127 141 155 169 183 197 m/ Z I ' ' 1 ' I rt l i f ri . . । . . . . | r 43.10 69.40% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42196. Heptadecane, 2,6,10,15-tetramethyl- 57 71 5000 85 •m-1 n-' ' 31.40 31.60 31.80 32.00 32.20 m/z 71.05 61.45% 99 113 127 1 41 155 183 211 268 296 > • । > ■ ■ * । *111 TTITTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ■Abundance 43 57

71 . #71191: Heptadecane . A. 31.40 31.60 31.80 32.00 32.20 5000 m/z 85.10 39.13% 85

1. 99113 127 141...................... 240............... ,

m/z-> Abundance 40 ' ■ i' ■' • i ■ ■ ■ ■ i'

60 43 5 7 80 100 120 140 160 180 200 #71948: Nonadecane 220 240 260 280 300 . A.. 31.40 31.60 31.80 32.00 32.20 m/z 55 05 23.52% 71

m/z--> 5000

I 'II ■ ■ । • ■ ■ ■ । 40 60 80 85

_ 113 127 . ... . 210 225 100 120 140 160 180 200 220 240 260 268. .. 280 300 N 1—IIIIIIT ' ytv । TT 11 । 31.40 31.60 31.80 32.00 32.20

27009.D NP112701.M Tue Dec 11 14:59:35 2001 Page 7

NYC-WTC_000032547

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NYC-WTC_000032547Source: NYC Law Department, mirrored locally

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