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GC/MS analysis results for sample AD22558, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS ' Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heptadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

34.76 0.62 ng/uL 82856 Chrysene-dl2 33.29

Hit# of 5 :ntative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 78 2 Hexane, 2,3,3-tetramethyl- , 142 C10H22 013475-81-5 50 3 Hexade c^ne 226 C16H34 000544-76-3 38 4 Ether,/heptyl hexyl 200 C13H28O 007289-40-9 37 <\bundance Scan 3263 (34.756 min): 22558.D (-) m/z 57.10 100.00% 57 43 71 5000 85

Ti/z-> ^bundance 40 u 60 80 1 99 II.................... 207 100 120 140 160 180 200 220 ■ 240 34.40 34.60 34.80 35.00 m/z 43710 71.44% #71191; Heptadecane 57 43

71 5000 85 34.40 34.60 34.80 35.00 m/z 71.05 63.40% 3/ 113 127 141 ,, ........................................... 240 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #8106: Hexane, 2,2,3,3-tetramethyl- 43 57 I ' ' I ' I ' 34.40 34.60 34.80 35.00 85 m/z 85.05 42.29%

71 , I,I , ,| , , | ,,, 99 J..... n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #70789; Hexadecane 5(7 34.40 34.60 34.80 35.00 43 m/z 55710 28.74% 71 5000 85

il 113 127 226 ^0 240 tt/z-> 40 60 80 100 120 140 160 180 200 34.40 34.60 34.80 35.00

22558.D NP072501.M Mon Oct 01 14:52:42 2001 Page 13

NYC-WTC_000087117

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