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GC/MS analysis results for sample AD22558, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\SEP2701\22558.D vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexacosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 35.65 0.53 ng/uL 62076 Perylene-dl2 ' 37.40 Hit# of 5 Tentative ID MW MolForm CAS# Qual

^Hexacosane 366 C26H54 000630-01-3 83 2 Tetratetracontane 619 C44H90 007098-22-8 83 3 Heptacosane 380 C27H56 000593-49-7 83 4 Tetratriacontane 479 C34H70 014167-59-0 72 Abundance Scan 3360 (35.646 min): 22558.D (-) m/^ 57.10 100.00% 57

5000 85 ' ' I ' ' 35.40 35,60 35,80 36.00 m/z43710 60.32% tVz-> 5o' i(^ " 150 ' ' 2(^ ' ' 250 " 3(TO ' 3^ " 400 " 4^ ' ' 5(^ " 5^ " 600 Abundance #51010: Hexacosane 57

5000 85 35.40 35.60 35.80 36.00 m/z 71.05 58.26% (Tu, I... .......... ....... .. •nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Wjundance #61068: Tetratetracontane 57 ft 35.40 35.60 35.80 36.00 5000 m/z 85.05 33.21% 85

. I.... . , . , I , , , I.... TT/Z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #52248: Heptacosane T 57 35.40 35.60 35.80 36.00 m/z 55.10 30.02% 5000 85

i f i J. f I . 380 Tl/z-> 50 100 150 200 250 300 350 400 450 500 550 600 35.40 35.60 35.80 36.00

22558.D NP072501.M Mon Oct 01 14:52:45 2001 Page 14

NYC-WTC_000087118

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