GCMS results log, sample AD26833, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Tetracosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

35.54 2.11 ng/uL 609193 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Tetracosane 338 C24H50 000646-31- 91 2 Hexatriacontane 507 C36H74 000630-06- . 9 3 Pentacosane 352 C25H52 000629-99-2 9 4 Eicosane 282 C20H42 000112-95-8 87 'Abundance Scan 3348 (35.545 min): 26833.D (-) m/ z 57.10 100.00% 57 43 71 5000 85

Tr 35.20 35.40 35.60 35.80 — - j 99 113127141155 ....... 281 m/ z 43.10 It | . < I . | I . < . | . t I | 'I' 68.93% 'm/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 EPYTTP T IT ! —35.20 35.40 35.60 35.80 : 99 m/z 71.05 56.26% : ‘ I‘ J | 113127 155169183197 I' ' ' 'T 294 ■ ■ ■ i I1 ' 1 * I ' 338 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

71 5000 85 m/ z 85.15 42.17%

! m/z-> 40 —.. m 100 99 113127141155169183197211

60 120 140 160 180 200 220 240 260 280 300 320 340 80 I I | i > < ■ | I TIITEET I | I ! ! I | T‘

Abundance #73718: Pentacosane 11 M4 TT ■ ।■ ■ ■ • । • ■ ■ ■ । ■ । ■ 43 57 35.20 35.40 35.60 35.80 m/ Z 55.10 24.12% 71 5000 85

99 l 113127141 155169183197211225 WAAMA4— i 1' I'11' I' TIhl ‘ I ' ’' ' I' '’'I I' '' 'I•'''I'''*I’'' ' I TTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

26833.D NP112701.M Tue Dec 11 14:46:53 2001 Page 12

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