GCMS results log, sample AD26833, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Pentacosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.66 2.44 ng/uL 809733 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Pentacosane 352 C25H52 000629-99-2 90 2 Heptacosane 380 C27H56 000593-49-7 90, 3 Dotriacontane 451 C32H66 000544-85-4 87 4 Hexadecane 226 C16H34 000544-76-3 86 Abundance Scan 3252 (34.664 min): 26833.D (-) m/z 57.10 100.00% 57

5000 85 11,7/T/T I ' ' 1 1 1 ' 34.40 34.60 34.80 35.00 I J I 113.141 , 183 207 m/z 43.10 62.25% m/z-> 50 100 150 200 250 300 350 400 450 ‘Abundance #49559: Pentacosane 43 t ! 71 5000- TTPPTmpet 34.40 34.60 34.80 35.00 m/z 71.05 58.48% s I 127 99 I 197 225 253 325 352 ’ 0- 100 150 200 250 300 350 400 450 m/z--> 50 Abundance #74082: Heptacosane ! 43 Tfr 71 34.40 34.60 34,80 35.00 5000 m/z 85.05 40.95%

99 127 1 I I rk 183 211 253 353 380 m/z--> 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane 57 34.40 34.60 34.80 35.00 m/z 55.10 24.18% 5000- 85

i 1113.141 1 1 1 f 1 1 ' I 196 281 422 450 4-44-4-4 । . —Pp m/z-> 50 100 150 200 250 300 350 400 450 34.40 34.60 34.80 35.00

26833.D NP112701.M Tue Dec 11 14:46:50 2001 Page 11

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