GCMS results log, sample AD26988, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File G:\HPCHEM\1\DATA\DEC0 6 01\26988.D Vial: 15 Acq On 6 Dec 2001 10:54 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Tetracosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD■ R.T.

33.75 0.41 ng/uL 122845 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qu

1 Tetracosane 338 C24H50 000646-31-1 (86 2 Heptacosane 380 C27H56 000593-49-7 78 3 Pentacosane 352 C25H52 000629-99-2 78 4 Hexadecane 226 C16H34 000544-76-3 72 Abundance Scan 3152 (33.746 min): 26988.D (-) m/ z 57.10 100.00%] I 57

5000- 85 4 A • ’ i •

m/z-> ‘I‘ TT" 40 60 4+ 4 . 113 i • " •i " ” i 207 226 j । । • p " । | "

80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 | । ' « • ! . । | । । | । । | ’ I * " • | 33.40 33.60 33.80 34.00 m/ z 4 3.10 64.99% Abundance #73543: Tetracosane E7

5000 85 -4— — ----- 33.40 33.60 33.80 34.00 m/z 71.05 . 59.08% U 1113 rp-rrrp-r 155 I' • 183 I >»111" ’' I' 1111 T’TTTT 294 i ■ ■ ■ ■ i 338 i " ’11 ■ r *1 • i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74082: Heptacosane 1 43 —A TT ' 71 33.40 33.60 33.80 34.00 5000 m/z 85.0,5 45.37% I ! । 99 127 i 183 211 253 353 380 TT‘ I TTTn 111" I 11 • ■1111' " i " 1111 TTTT T‘UT"ITTTT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #49559: Pentacosane IT 43 33.40 33.60 33.80 34.00 m/ z 55.10 29.72% 71 5000

0 1' I11 £ M 99 , 127 197 225 253 325 352 —MM ....... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 33.80 34.00 33.40 33.60

26988.D NP112701.M Tue Dec 11 14:53:42 2001 Page 5

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