GCMS results log, sample AD26987, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\1\DATA\DEC0601\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Tetracosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

29.70 0.77 ng/uL 230883 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetracosane 338 C24H50 000646-31-1 6 2 Heptadecane 240 C17H36 000629-78-7 6) 3 Pentadecane 212 C15H32 000629-62-9 80 4 10-Methylnonadecane 282 C20H42 000000-00-0 72 Abundance Scan 2711 (29.700 min): 26987.D (-) m/ z 57.10 100.00% t

43 57 71 5000- 85

99 ' ■ I ■ ' ' ' I ' ' ' ' TIIEE

m/z-> 40 41113127141155, 60 80 । । . , , , j-ri . i p . . . । . . . . । 100 120 140 160 180 200 220 240 260 280 300 320 340 ■p 29.40 29.60 29.80 30.00 m/z 43 . 10 74.55% Abundance #73543: Tetracosane 43 57 71

85 )8 5000 TT 29.40 29.60 29.80 30.00 99 m/z 71.05 59.72% J 113127 155169183197 294 338 ‘ I"‘ESI-TEII‘I ITTT I1 1 ' 1 I i11'11' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71191: Heptadecane 43 57 ' ' 1 * 1 TE""TI 71 29.40 29.60 29.80 30.00 5000- m/z 85.15 40.70% 85

99 113127141 240 miz-> 40 60 80' 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #70278: Pentadecane A | A . < I ! | I I • • | ' ' J ’ ' 43 57 29.40 29.60 29.80 30.00 m/ Z 41.10 26.68% 71 5000 85

| । , 99 1)3127141155169 212 '' i' ■'' i''" ’ i"''' 1111 ■ i ■ ■' ■ (■' ■i' " ' i ■ ■ ■ ■ r ■1 ■ i ■ ■' ■ r ' ■ ■ i1 ■'' r ' ■ ■ i ■ ■ ■' i ■ ■' ■ i' - P—PPP- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 29.40 29.60 29.80 30.00

26987.D NP112701.M Tue Dec 11 14:52:48 2001 Page 4

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