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GCMS results log, sample AD26987, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26987 completed on December 11, 2001.

NYC-WTC_000032427–000032447

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Eicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.77 1.00 ng/uL 300607 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 91 2 Heptadecane 240 C17H36 000629-78-7 90 3 Pentadecane 212 C15H32 000629-62-9 86 4 Tetracosane 338 C24H50 000646-31-1 86 Abundance Scan 2828 (30.773 min): 26987.D (-) m/z 57.1.0 100.00% 57 43 71 5000 85 / Tii I ' 1 ' TT 30.40 30.60 30.80 31.00 31.20

m/z--> J ■ ' T ' 40 —l+ 99 113 127 141 60 80 TT-———-----TTTTDTOTDRTPTTTTFTTTT 100 120 140 160 180 200 220 240 260 280 m/z 43.10 68.62% Abundance #72323: Eicosane 43 57

71 - I 5000 TI Ir 85 30.40 30.60 30.80 31.00 31.20 m/z 71.0,5 64.04% > 11' ■ w-n 1— 22 113 127 141 282 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 — 1 71 30.40 30.60 30.80 31.00 31.20 5000 m/z 85.05 • 39.12% 85

, ' ‘ 99 TImmmmm—TT 113 127 141 240 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #70278. Pentadecane 43 57 30.40 30.60 30.80 31.00 31.20 m/z 41.1,0 30.09% 71 5000 - 85

99 113 127 141 155 169 212 • i > ■ > > i ■ • ■ • i > m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 30.40 30.60 30.80 31.00 31.20

26987.D NP112701.M Tue Dec 11 14:52:50 2001 Page 5

NYC-WTC_000032439

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NYC-WTC_000032439Source: NYC Law Department, mirrored locally

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