GCMS results log, sample AD26987, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.71 1.99 ng/uL 7362 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetradecano e (myristate) 284 C18H3602 000000-00-0 72 2 Cyclopentanecarbo! ylic acid, 2-amin 129 C6H11NO2 040482-05-1 43 3 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 43 4 Octadecanoic acid, 2-methylpropyl e 340 C22H4402 000646-13-9 42 Abundance Scan 2930 (31.708 min): 26987.D (-) m/ z 56.1.0 100.00% 56

5000 4 73 , , ।, , , , । ,< . . । rr; i । . .. . । 97 .=129 267 285 31.40 31.60 31.80 32.00

miz-> L 41 — I' ' ' 1 T1 20 40 60 T‘ 185 241 TPTT r 1' TT 340 11 80 100 120 140 160 180 200 220 240 260 280 300 320 340 | m/z 57.10 53.16% Abundance #40186: Butyl tetradecanoate (myristate) 55

5000- 229 31.40 31.60 31.80 32.00 73 211 m/ z 43.10 42.66% 129 185 284 101 L | f I i1'1' i11' r rr Tn I'1'' I TTIT • । ■ ■■■। ■• ■•।■ ■ ■ ■ । miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5212: Cyclopentanecarboxylic acid. 2-amino-. trans- 56

31.40 31.60 31.80 32.00 5000- m/z 41.10 37.21%

30 82 100 129 । ■ ■ • ■ । । ■ i' p-m-p-m-r I ’ ' ' T‘ ‘TT r■••i i' •111 r "' i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino, cis- / I"r 11 56 31.40 31.60 31.80 32.00 m/ z 55.10 31.48% 5000

30 82 100 129 J i''' • i ■ , >1) T’TTTT t J prCTTp-rTTTTTTTpnrn-TYrn^^ 11 ■'' i''' ■ r ■ ■' i''' ■ i'1 • ■ i 1 ■ ■ ■ । ■ ■ ■ ■ । ■ ■ TTfr r i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

26987.D NP112701.M Tue Dec 11 14:52:52 2001 Page 6

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