GCMS results log, sample AD27009, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.71 3.01 ng/uL 1336180 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetradecanoate (myristate) 284 C18H3602 000000-00-0 (80 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11N02 040482-05-1 43 3 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 43 4 Decane, 2,2,3-trimethyl- 184 C13H28 062338-09-4 38 Abundance Scan 2930 (31.709 min): 27009.D (J m/ z 56.10 100.00% 56

5000 - 4 73 ............ 4 — —....... . —i miz-> 20 40 60 14712 4 157 185199 97 129 I ■ ■ • ■ i 80 100 120 140 160 180 200 220 240 260 280 300 320 340 .. 241 TWWIu 22= °7 285 [ 340 II 31.40 31.60 31.80 32.00 m/z 57.10 51.61% 'Abundance #40186: Butyl tetradecanoate (myristate) 56 1 i ■ 7 I ' 1 ' ■ i 5000- 229 31.40 31.60 31.80 32.00 73 129 211 m/z 43.10 44.20% 185 284 111111 "1111 101 1 I____ i ■'' ■ i r ■ ■ ■ i'" ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-. trans- 56 i 1 ' ■ 1 i 31.40 31.60 31.80 32.00 5000- m/ Z 41.10 36.19%

30 82 100 129 i ■ ■'' i ■''' i i' ''' i i •'' ■ i''1' i ‘ ■ i' ' i i ■ ■ ■ ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- 11T _ ■j-T-r

56 31.40 31.60 31.80 32.00 m/z 55.10 30.83% 5000

30 82 100 129 | _ ■ )

1 1 1. I i' " ■ i' ri -1« । ■ ■ ■ ■i• ■■ ■। >i■ ■ ■ ■ ।■ •■ < । • i l ■' ‘ ■ i i ■ • ■ ■ i ■ • ■ ■ । i I 1 ' Trt l m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

27009.D NP112701.M Tue Dec 11 14:59:33 2001 Page 6

NYC-WTC_000032546