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GCMS results log, sample AD27009, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27009 completed on December 11, 2001.

NYC-WTC_000032534–000032552

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032545
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title ■ : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Eicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.77 1.01 ng/uL 449521 Chrysene-dl2 33.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 2 Nonadecane 268 C19H40 000629-92-5 90 3 Docosane 310 C22H46 000629-97-0 90 4 Tetracosane 338 C24H50 000646-31-1 87 Abundance Scan 2828 (30.774 min): 27009.D (-) m/ z 57.10 100.00% 43 57 71 5000- 85

30.40 30.60 30.80 31.00 31.20 113 127 141 155( LD 29TTTT ' ■ T 1 ' '11111 r1 । । । । ji m/z 43.10 71.64% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72323: Eicosane 43 57

71 5000 TIr TT—meTETTerrm 85 30.40 30.60 30.80 31.00 31.20 m/z 71.05 64.25% ! : ■ . | ,

। . . । . । . i । । r I: T. 113 127 141. .... ......... 2 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ’Abundance #71948: Nonadecane 43 57 T IT 71 30.40 30.60 30.80 31.00 31.20 5000 85 m/z 85.15 41.19%

99 113 127 156 196210 225 268 1 1 i 1'1 * i ' 1 1 ' i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72997: Docosane ‘I T8 4(3 57 30.40 30.60 30.80 31.00 31.20 m/ z 41 • 10 27.07% 71 5000- 85

-— 29 113 127 155169183 197 211 292 310 L44444 • i'1'' । *'' * ।' ■ ■ । ■ ■ ■ ■ । i • • ■' I 4 14'14 i m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30.40 30.60 30.80 31.00 31.20

27009.D NP112701.M Tue Dec 11 14:59:30 2001 Page 5

NYC-WTC_000032545

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NYC-WTC_000032545Source: NYC Law Department, mirrored locally

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