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GCMS analysis results for sample AD26626, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26626 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031940–000031967

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Eicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.81 1.25 ng/uL 281263 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 2 Hexatriacontane 282 507 C20H42 C36H74 000112-95-8 000630-06-8 91 92 212 C15H32 3 Pentadecane 4 Nonadecane Abundance Scan 2941 (31.808 min): 26626.D (-) 268 C19H40 m/ z 57.10 000629-62-9 000629-92-5 100.00% 87/ 57 43 71 5000 85 i ■ ■ • ■ i ■ ■

A +4 1113,127 141 99 413 31.40 31.60 31.80 32.00 32.20 —1 m/z 43.10 68.87% m/z-> 40I 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57 71 TTTmT 5000 85 31.40 31.60 31.80 32.00 32.20 I m/z 71.05 63.47% ! I I m/z-> 1 1, I ■ T i ■ • ‘ ‘ i ■ • 40 60 + 100 80 99113/127 141 ....................... ........ . 120 140 160 180 200 220 240 260 280 'Abundance #74636: Hexatriacontane 43 57

71 M 4..... . 1 1 31.40 31.60 31.80 32.00 32.20 5000- 85 m/z 85.05 41.46%

97 _ / ■ 113 127 141 155 169 183 197 211 m/z-> Abundance 40

57 60 80 100 120 140 160 180 200 #26001: Pentadecane 220 240 260 280 4 31.40 31.60 31.80 32.00 32.20 43 71 m/ Z 41.. 10 23.00% 5000 85

99 4 10

> ■ i > • l ' ' 11- „I 113 127 168 212 ■ • i ■ ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.40 31.60 31.80 32.00 32.20

26626.D NP112701.M Fri Dec 07 14:50:28 2001 Page 16

NYC-WTC_000031961

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NYC-WTC_000031961Source: NYC Law Department, mirrored locally

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