GCMS results log, sample AD27008, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\1\DATA\DEC0601\27008.D Vial: 21 Acq On 7 Dec 2001 4:21 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Eicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.81 0.52 ng/uL 165999 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 (86. 2 Tetradecane 198 C14H30 000629-59-4 64 3 Ether, heptyl hexyl 200 C13H280 007289-40-9 47 4 Hexane, 2,2,3,3-tetramethyl- 142 C10H22 013475-81-5 47 Abundance Scan 2941 (31.809 min): 27008.D (-) m/z 57.10 100.00% 57 43 71

5000 85

I."T TIIIT

1 l 99 31.40 31.60 31.80 32.00 32.20 — m/ z 43.10 78.65% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57 71 5000 It" ■ > i ■ ■ 85 31.40 31.60 31.80 32.00 32.20 m/z 71.05 70.44% Ii _l "d."II T T-r-rTT"T-r ‘ , n- 99 113 127 141................... .............. 282 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69661: Tetradecane 57 43 .. A — .. — 71 31.40 31.60 31.80 32.00 32.20 5000 m/z 85.15 44.87% 85

27 99 113 I 155 198 .m/z->__ 20__ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #23013: Ether, heptyl hexyl - A---... 43 57 31.40 31.60 31.80 32.00 32.20

m/z-> 5000

20 27 . i 40 I i ■ ■ ' ■ i ■ ' 60 70 | 85

ll 80 97 115 100 120 140 160 180 200 220 240 260 280 m/ z

1‘I M 41.05 31.52%

■ i ■ • 31.40 31.60 31.80 32.00 32.20

27008 .D NP112701.M Tue Dec 11 14:58:06 2001 Page 4

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