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GCMS results log, sample AD26987, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26987 completed on December 11, 2001.

NYC-WTC_000032427–000032447

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032441
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987 .D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Heptadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.80 2.57 ng/uL 768881 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 (91) 2 Tetracosane 338 C24H50 000646-31-1 90 3 Nonadecane 268 C19H40 000629-92-5 90 4 Nonadecane 268 C19H40 000629-92-5 87 Abundance Scan 2940 (31,800 min): 26987.D (-) m/z 57.10 100.00% 57

43 71 5000- 85

I • TT ’ I ' 1 ■ i ' ' ' M ' ' ' ' I ' ' Ji *2 113127141 155169183 — , TTT 31.40 31.60 31.80 32.00 32.20 TTT . "T . , T. । . . . . f . . , , । , J . . , . . . , । , . i I । , , , . । , , I , । I i . . | I I i i । , , , . । , , , , । . m/ z 43.10 68.63% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance

; 5000 - 43 57 71

85

. . । . . . . । . . . . । 'i 99 113127141 #71191: Heptadecane

240 M 31.40 31.60 31.80 32.00 32.20 m/ z 71.05 59.67% 11' ■ ' ■ i1 ■ ■ ' i ■ •' ■ i' '111 ■'' ■ i ■ ' ■' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i ■ ■ ' ■ i ■ ■ ■ ■ i'

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 TE" ■ ' i ■ • 31.40 31.60 31.80 32.00 32.20 5000- 85 m/z 39.67% 99 I 113127155169183197 294 338 1 11 1 ’ ‘ I 1 1 1 ' I ' i11111 ' ’ • I ' ‘’ I ' TT i ■ " ' i •'111''1 ‘ i ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71948: Nonadecane TIT ■ ' i ■ ' 43 57 31.40 31.60 31.80 32.00 32.20 m/z 41.10 25.38% 71 5000 85

99 113127 156 TT-n— TT‘tE‘11E1-0———-I-ETTI"TEITETETTEIE‘TIIIITOO—11——TTim 196210225 268 ‘I1" m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 3140 31.60 3t80 32.00 32.20

26987.D NP112701.M Tue Dec 11 14:52:54 2001 Page 7

NYC-WTC_000032441

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NYC-WTC_000032441Source: NYC Law Department, mirrored locally

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