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GCMS results log, sample AD27012, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27012 completed on December 11, 2001.

NYC-WTC_000032575–000032586

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032585
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27012.D Vial: 20 Acq On 7 Dec 2001 3:27 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Eicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.80 0.41 ng/uL 149155 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 59 2 Pentadecane 212 C15H32 000629-62-9 56 3 2,6-Dimethyldecane 170 C12H26 013150-81-7 45 4 Hexane, 3,3,4-trimethyl- 128 C9H20 016747-31-2 43 Abundance Scan 2940 (31.804 min): 27012.D (-) m/z 57.10 100.00% 57 43 71

5000 85

TIT ' ■ i ' ' 99 113 31.40 31.60 31.80 32.00 32.20 1 11 1 m/ z T T । . . . . । , TTIT r i >■ I | I I 75.85% m/z- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57

71 5000 - TI" ‘ ■ i ■ ■ 85 31.40 31.60 31.80 32.00 32.20 m/z 71.05 74.74% i | I,___III 99 113 1 27 144 282 i ' ■ ■ ' i ■ ' ' 1 i ' ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #70278: Pentadecane 1 I i 43 57

71 —... AA 31.40 31.60 31.80 32.00 32.20 5000 85 m/z 85.05 44.10%

: 1 99 113 127 141 155 169 212 'm/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #15357: 2,6-Dimethyldecane .............. ......................... .. , 43 57 31.40 31.60 31.80 32.00 32.20 71 m/z 41.10 30.24% 5000 85

27 , 113

m/z-> 20 1 1 1 1 1 1 ’ 40 — 60 80 — 100 120 140 160 170 180 200 220 240 260 280 I"T A 31.40 31.60 31.80 32.00 32.20

27012.D NP112701.M Tue Dec 11 15:00:35 2001 Page 3

NYC-WTC_000032585

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NYC-WTC_000032585Source: NYC Law Department, mirrored locally

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