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GC/MS analysis results for sample AD22653, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087320
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\l\DATA\SEP2801\22653 Vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101 M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************.-.•*.,******************** Peak Number 11 Pentacosane Concentration Rank 6 R.T. EstConc Area Relative; to ISTD R.T. 34.64 0.75 ug/1 111676 Chrysene-c ' 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25n52 000629-99-2 91 2 Tetratetracontane 619 C4- H9 0 007098-22-8 91 3 Hexadecane 226 C16H34 000544-76-3 90 4 Heneicosane 296 C2- T-; t 000629-94-7 90 Abundance Scan 3224 (34.640 min); 22653.D (-) Hi? 57.00 100.00% 5(7

5000 85

34.40 34.60 34.80 35.00 .................. m/z 71.05 75.56% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73718: Pentacosane 43

71 5000 _ 34.40 34.60 34.80 35.00 m, . 43.0.5 71.32% 99

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #61068: Tetratetracontane 57

34.40 34.60 34.80 35.00 5000 m/;'. 85.05 47.70% 85 A ■ , 379407 530013 Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 500 Abundance #29267: Hexadecane 57 ___ 34.40 34.60 34.80 35.00 • m/z 41.00 26.39%

55S 85

1962^ Tl/z-> 50 100 150 200 250 300 350 400 450 500 550 34.40 34.60 34.80 35.00

22653.D NP091101.M Fri Oct 05 08:57:03 .' OCl Page 11

NYC-WTC_000087320

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NYC-WTC_000087320Source: NYC Law Department, mirrored locally

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