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GC/MS analysis results for sample AD22653, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Repo.,

Data File : C:\HPCHEM\l\DATA\SEP2801\22653J- Vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.m (RTE integrator) Title : 209 625/TCLP calibration tab 7/16, .1 Library : C:\DATABASE\NBS75K.L *********************************************- ■ r***.' ir***************

Peak Number 12 Eicosane Concentration Rank 7 R.T. EstConc Area Relativ - I EID R.T. 35.53 0.74 ug/1 101310 Peryleno- 37.28 Hit# of 5 Tentative ID MW Me : ? irm CAS# Qua! <,1) Eicosane 282 C:Y . (: 000112-95-8 93 ^2 Heptadecane 240 Cl' 111 000629-78-7 91 3 Tetratetracontane 619 C4/ -T 0 007098-22-8 90 4 Hexatriacontane 507 C3i 000630-06-8 90 Abundance Scan 3321 (35.531 min): 22653.D (-) m, ?, 57.00 100.00% 57

5000 85

_3 ■:20 35.40 35.60 35.80 m, ■■ 43.00 65.79% 50 100 150 200 250 300 350 400 450 500 551 Abundance #72323: Eicosane 57

5000- '20' '3'5'40 3'5.60 '3'5.80 85 71.1063717% 282 A mZz-> 50 100 150 200 250 300 350 400 450 500 55: Abundance #32063: Heptadecane 57

85 .20 35.40 35.60 35.80 5000- I. 85.05 43.86%

r-n-p Tife-> 50 100 150 200 250 300 350 400 450 500 550 500 Abundance #61068: Tetratetracontane 57 20 35.40 35.60 35.80 z 55.00 24.48% 5000 85 I 160 150 " 2(^ ' 250 " 300 ' ' ^0 400 " ^ " ^ " 550 T 50 : ^.20 35,40 35.60 35.80

22653.D NP091101.M Fri Oct 05 08:57:06 Page 12

NYC-WTC_000087321

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NYC-WTC_000087321Source: NYC Law Department, mirrored locally

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