Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Eicosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 35.53 0.74 ug/1 106189 Perylene-dl2 37.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual (^Eicosane 282 C20H42 000112-95-8 93 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Tetracosane 338 C24H50 000646-31-1 91 Abundance Scan 3321 (35.532 min): LBE.D (-) m/z 57.00 100.00% 57 71 43 85 5000
UL 99 35.20 35.40 35.60 35.80 Yt-T .-,4,, . A |T 7^ .'',^1 I,, ....... . ^^^1,.. mZz 71705 767^8% ■n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72324: Eicosane 43 5(7
71 5000 “ ■'TTYTT'riTf. , fm'TYrrr'rj' 85 35.20 35.40 35.60 35.80 m/z 43.05 64773%
I ' ' I J ?1P 141 155 169 183 197 254 282
I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #74636: Hexatriacontane 43 57 “H” 71 35,20 35,40 35.60 35.80 5000 85 m/z 85.05 51.75%
97
tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73718: Pentacosane 43 5,7 35.20 35.40 35.60 35.80 Wz 54.95 26.68% 71 5000 85
■n/z-> 40 u60 80 /L 100 120 140 160 180 200 ???, 220 240 260 280 35.20 35.40 35.60 35.80
LBE.D NP091101.M Wed Oct 03 14:41:28 2001 Page 16
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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