Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM \1\DATA\OCT0101\LBE.D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Heneicosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 34.64 0.90 ug/1 145324 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Heneicosane 296 C21H44 000629-94-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Nonacosane 408 C29H60 000630-03-5 91 Abundance Scan 3224 (34.641 min): LBE.D (-) m/z SYTOO 100.00% 57 43 71
5000 85
99 T"^ J .Jl, III 169 183196 211 34.40 34.60 34.80 35.00 Y-r4*tnrY1VT^t‘Y'rT'T^-j-f‘VTTjS-r-rVp-|H-rTVTr-r+j-rT-*T-p-r^^ m/z 71.10 70.89% -n/iz-> 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 pt i-i I-/ I h-r r r-<T^' 5000 34.40 34.60 34.80 35.00 99 m/z: 43.00 65.22% J, ll .............................. 268 296 ■n/z-> 40 60 80 100 120 140 1^ 180 ^0 240 260 280 3CX3 Abundance #74636; Hexatriacontane 43 5(7
71 34.40 34.60 34.80 35.00 5000 85 m/z 85.05 48.50%
97
■n/z-> 40 60 J 80 IJ ■’27 141 155169 183197 211 . . I r I I I I I 1 .-| f I I I ■. I . . 1 I « . I I . . . I I 100 120 140 160 180 200 220 240 260 280 300 I ' ' ‘ H '
Abundance #32063; Heptadecane iQ T 57 34.40 34.60 34.80 35.00 71 m/z 55.00 24.25% 85 5000
99
■n/z-> 40 u. J T’F’f 60 80 240 -d-r I'''' I 100 120 140 160 180 200 220 240 260 280 300 196 34.40 34.60 34.80 35.00
LBE.D NP091101.M Wed Oct 03 14:41:26 2001 Page 15
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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