Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T. 33.71 1.44 ug/1 233381 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Tricosane 324 C23H48 000638-67-5 91 Abundance Scan 3123 (33.714 min): LBE.D (-) m/z SYTOO 100.00% 57
5000 85
-r-T-p-r-n-r-r L T jYjVfyiJS 197 227 253 281 33.40 33.60 33.80 34.00 .1 Wz 71.10 71.55% ■Tlfe-> Abundance 50
57 100 150 200 250 300 350 #59136: Hexatriacontane 400 450 500
I 5000 85 33.40 33.60 33.80 34.00 m/z 43.05 64.54% \ (1 j J** 1^1,'If'* ,,, , I,, . . . ........... rA-> 50 100 150 200 250 300 350 400 450 500 Abundance #71193: Heptadecane c7
33.40 33.60 33.80 34.00 5000- in/z 85.05 47773% 85 I J^P,141 169 210 240 ' I ' ' ‘ ' I ' ' ' ‘ I ' ' ' ' I ' n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #51002: Heneicosane, 11-(1-ethylpropyl)- r’-'' '-■-1 I 43 33.40 33.60 33,80 34.00 m/z41.05 24.44% 71 5000
I II J 183 J^5......... 2^^ 3^........................................ ■n/z-> 50 'l6o ' 'l^ 200 250 ' 300 ' 350 ' ' '460 ' 4^ ' ' 'sOO ' 33.40 33.60 33.80 34.00
LBE.D NP091101.M Wed Oct .03 14:41:24 2001 Page 14
NYC-WTC_000087151
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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