Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
NYC-WTC_000087496–000087516Folder label: “GC/MS Scan 9/20/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0 2 01\LB.D vial: 2 Acq On 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample 9/20 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 30.73 0.55 ug/1 84270 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Heneicosane 296 C21H44 000629-94-7 90 4 Tetracosane 338 C24H50 000646-31-1 90, Abundance Scan 2799 (30.733 min): LB.D (-) m/z 57700 rOOTOO‘% 57
5000 85
T I I 30.40 30.60 30,80 31.00 ,141 169.................................. m/z 43.05 70.83% tVz-> Abundance 50
57 100 150 200 250 300 #59136: Hexatriaconlane 350 400 450 500 I 5000 I'l |*i I ,*i"pr 1 1 I i" “r7 I r r I 85 30.40 30.60 30.80 31.00 m/z 71.00 6^773% A -I—r-|—r-r 379 407 435 478 506 ■n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #71193: Heptadecane 5^ Ik 30.40 30,60 30.80 31,00 m/z 85.05 47.07% 85
n/z-> ' ' I ' 50 .100r? 150 200 250 ............ 300400 450 350500 \ Abundance #42201: Heneicosane ' ' 'I 57 y.40 30.60 30.80 31.00 m/z 41.05 25737% 85 5000
..... ........................ WA AQ 50 100 150 200 250 300 350 400 450 500 30,40 30,60 30,80 31.00
LB.D NP091101.M Wed Oct 03 10:09:57 2001 Page 7
NYC-WTC_000087508
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086981
Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
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NYC-WTC_000087492
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.
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