Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
NYC-WTC_000087496–000087516Folder label: “GC/MS Scan 9/20/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document xjj.jjici±Y oearen compouna Report
Data File C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On 2. Oct 2001 3:06 pm Operator: 2 09 GTkLOS Sample 9/20 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclopentanecarboxylic acid, 2 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.54 1.71 ug/1 260921 Chrysene-dl2 33.16 Hit# of 5 y Tentative ID MW MolForm CAS# Qual
1 Cycloperitanecarboxylic acid, 2-amin 129 C6H11NO21 040482-05-1 38 2 Cyclobi/tane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 3 Cyclobutane, l-hexyl-2,3-dimethyl- 168 C12H24 055170-84-8 35 4 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 Abundance / Scan 2669 (29.539 min): LB.D (-) pm/z 56.00 100.00% 53
5000 41 73 257 II q? 129 239 I 29.20 29.40 29.60 29.80 , .ll. A .7,'. A”??, ..t ■ ■ I,., ■ ....... . 312 m/z 57.00 50.25% 1l/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 5
c553 29.20 29.40 29.60 29.80 m/z 41.05 36704% 30 ,1 , tVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 53 I i-i .9t i"| . Z k/V.Ti'. 9-r. p 29.20 29.40 29,60 29.80 53 m/z 43.05 34791%
27 70 I I, I, 9/ 111125140 168 196 rr^T-f4‘-rTlY'T-VT-|T-TTr1n-rT-^^ I'' '' I ‘' I''' ' I''' ' I'''' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #14719: Cyclobutane, 1-hexyl-2,3-dimethyl- 53 29.20 29.40 29.60 29.80 m/z 73700 28.18% (1 5000
70
Tl/z-> 42 I I' ' '' I ' 20 40 Ux 60 ^8 112'126 ’' I'''' I'''' I r ' • ’ I'''' r ‘' I'' ‘' I 80 100 120 140 160 180 200 220 240 260 280 300 p-m-p-r-rry I 29.20 29.40 29.60 29.80
LB.D NP091101.M Wed Oct 03 10:09:55 2001 Page 6
NYC-WTC_000087507
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 2, 2001.
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