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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

.Data File C:\HPCHEM\1\DATA\OCT03 01\23080 .D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclobutane, 1,l-dimethyl-2-oc Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.53 1.82 ug/1 262461 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclobutane/ 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 2 1 -Hexene, /5- methyl - 98 C7H14 003524-73-0 27 3 1-Hexene/ 2-methyl- 98 C7H14 006094-02-6 27 4 Cyclob' ane, 1,2-diethyl-, trans- 112 C8H16 _ _019341398-1 27 'Abundance ( Scan 2667 (29.528 min): 23080.D (-) m/z 5 676 0 i 0 o'. "6 0 % 55

5000 41 73 129 257 ' ' I ' ' ' '1 ' ' ' ' I 'O' • JJ .Jb lltn .1 1431571711851992P ^39 | 29.20 29.40 29.60 29.80 312 H i I T I I fl I I tT I «■ I . . I I . 1 i'“j . I I I I I . I j I . I . I 1 ri q . I I Pj I I ' ' '7“| ri II I m/z 57.0.0 43.47% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985; Cyclobutane, 1,1^imethyi-2-octyl- 56

5000 A 29.20 29.40 29.60 29.80 27 m/z 36.44% I T I 111125140 168 196 ' ' ' I ' ' ' ' ' ' I " ' I I . . 'I , I , . , . I . . . . I I I 1 . I . . , . I , fn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63239: 1-Hexene, 5-mettiyl- 56 41 2020 2940 29.60 29.80 5000 m/z 43.05 35.76% 27 70 ..... ......... 98............... m/2->____ 20 40 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1 -Hexene, 2-methyl- 5(6 29.20 29.40 29.60 29.80 m/z 73.0.0 28.49% 41 5000 27 70 I 98 prT-TTrj-TTTT-p-TTTp-rnrTyT^^ /[ -T-rr tTl/Z~> 20 40 60 80 100 120 140 '160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23080.D NP091101.M Tue Oct 09 10:01:48 2001 Page 6

NYC-WTC_000087829

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NYC-WTC_000087829Source: NYC Law Department, mirrored locally

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