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Library Search Compound Report
Data File ; C:\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4
Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 6 Cyclobutane, 1,1-dimethyl-2-oc Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
29.50 4.55 ug/1 527857 Chrysene-dl2 33.12
Hit# Of 5 Tenfative ID MW MolForm CAS# Qual
1 Cyclobutai^ 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35
2 1 - Hexene 2 -methyl - 98 C7H14 006094-02-6 27
3 CyclobuXane, 1-hexyl-2,3-dimethyl- 168. C12H24 055170-84-8 25
4 Butyl/nexadecanoate_______________ 312 C2 0H40O2 _____ 000000-00-0 25
Abundance Scan 2665 (29.504 min); 23473.D (-) “m/z 56.00 100.00%
55
It
5000
41
73
T
.U 143157171185199213 j 29.20 29.40 29.60 29.80
312
111 1^ I I Pj I I T T I I II I j r'l r I I I I I I I I I I I '| I I I I I I '( I I J I TV Fj I m/z 5^795 47.33%
20 40 60 80 100 120 140 160 180 200 220 240 260 280 300
Abundance #21985; Cyclobutane, 1.1 <limethyl-2-cictyl-
5|5
5000
29.20 29.40 29.60 29.80
m/z 41.05 38.08%
nfe-> 20
27
I
40
70
I'' ■'
60
I It 9/ 111125140 1^
' I' •I' I ’''' I " '' I' I'' I''' ' I'
80 100 120 140 160 180 200 220 240 260 280 300
196
I '''' I'''' I'''' I'''' I'''' I
I
Abundance #1354; 1 -Hexene. 2-methyl- - ----------
53
1 ■ ■ I ■, J .vAa"
41 .^,20 2940 29,60 29^
5000 m/z 43.00 36.65%
27
■^- 98
I ' ' • I' •' ’ I p-TT-rp-TTT-pTTn-pnnnrpnTn-TTTT-T-pnTTyTT-T-rYr^^
Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300
(\bundance
53
#14719; Cyclobutane. 1 -hexyl-2.3-<iimethyl- ......... .iu
■ 29.20 29.40 29.60 -29.80-----
m/z 55.00 28.63%
5m
42
I
70
_ ___ l\j^„
j 1 I I I I I I . I j-. rr. I I I 1
I'''' I'''' r ''' I''' ‘ I'''' I
nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80
23473.D NP091101.M Wed Oct 17 13:17:34 2001 Page 6
NYC-WTC_000088737
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