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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088736
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NYC 9/11 Public Portal Document

a Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D Vial; 4 Acq On ; 16 Oct 2001 5;10 pm Operator; 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L *********************************************************************** Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.52 ug/1 51131 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dicl41orobenzene-d4 150 C6C12D4 003855-82-1 59 2 Benze:^-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 BenzaZLdehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-^8 10 no-2-chlorobenzonitrile _______ 152 C7H5C1N2 _______ 020925-27-3 9 Abundance Scan 717 (11.620 min): 23473.D (-) m/z 149.90 100.00% 1!i0

SOGO­ US S2 78 r'''' I ' ' I ' ' 40 11.20 11.40 11.60 11.80 12.00

Tife-> I" p " H " " 11 -HH-p-r 30 40 50 60 70 80 90 100 110 120 3^ 130 140 ISO 160 m/z 151.90 62732% Abundance #9693:1,4-Dichlorobenzene-d4 1!i0

sooo 11S 78 11.20 11.40 11.60 11.80 12.00 S2 m/z 114.90 35741% 35 ' I ' ' ' ' I ' ' ' ' I • ■n/z-> 30 40 50 60 70 80 90 ip0 110 120 1^ 140 ISO 160 ^bundance_____ _#9692:. Benzene-1,2,3,4-d4-, .6,6-dichloro- -— 1!i0

11S 11.20 11.40 11.60 11.80 12.00 SOOO S2 78 "niTz 77795 21797%

35 87 I I T 30 40 50 60 70 80 90 100 110 120 130 140 ISO 160 Abundance #66892; Benzaldehyde, 2-hydroxy-3-methoxy- _ 1$2 11.20-11.40 11.60 11.80 12.00- “m/z 52.00 17.96% 106 553 63 81-

122 92 136 I ' I ' ' ' ‘ I' ' ‘ ' I '' '' r ' I ' ' ' ' I”'”' ' ' I ' ' I ' -l-l I l-T n/z-> 30 40 50 60 70 80 90 100 110 120 130 ■ 140 160 160 11.20 11.40 11.60 11.80 12.00

23473.D NP091101.M Wed Oct 17 13; 17-.32 2001 Page 5

NYC-WTC_000088736

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NYC-WTC_000088736Source: NYC Law Department, mirrored locally

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