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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088219
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclobutane, 1,1-dimethyl-2-oc Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.51 6.89 ug/1 758548 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclobut^e, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 2 Butyl h^adecanoate 312 C2 0H40O2 000000-00-0 25 3 1,3-He/^ediol, 2-ethyl- 146 C8H18O2 000094-96-2 23 4 Oxiraj/e, 2,3-bis (1-methylethyl) - , t 128 C8H16O 054644-32-5 23 Abundance Scan 2666 (29.512 min): 23320.D (-) pm/z 56.00 100.00% 53

552 4' 73 257 L 239 " " I 312 29.20 29.40 29.60 29.80 -p. . I •''' I • ■ • ■ I ■ ■ I' I m/z 57.00 45.68% m&-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 5

5000 li ^.20 29.40 29.60 29.80 m/z 43.05 37.50% 27 70 I L 3/ 111125140 168 196 I ' ' ' ’ I ' I''' ‘ I ‘' I I''' ' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5

29.20 29.40 29.60 29.80 5000 258 m/z 41.00 35.45% 240 312 129 ...... 15^71 T 214 J I”''' ‘ I I'''' I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #66452:1.3-Hexanediol, 2-ethyl- ...... ................ 5b 29.20 29.40 29.60 29.80 m/z 73.00 31.66% 5000 73 (1 103

l,i. _____________ _ _ ___ __ _ .... . Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23320.D NP091101.M Mon Oct 15 09:53:43 2001 Page 6

NYC-WTC_000088219

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NYC-WTC_000088219Source: NYC Law Department, mirrored locally

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