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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088810
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NYC 9/11 Public Portal Document

— -Library-Search-Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclobutane, 1,l-dimethyl-2-oc Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.51 5.12 ug/1 620717 Chrysene-dl2 33.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual ■

1 Cyclobutan^ 1,1-dimethyl-2-octyl- 196 C14H28 ■ 062338-30-1 27 2 1-Hexene,/2-methyl- 98 C7H14 006094-02-6 27 3 Butyl h^adecanoate 312 C20H40O2 000000-00-0 25 4 1,3-He^nediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 4bundance / 50 Scan 2665 (29.506 min); 23499.D (-) Wz 56.00 - 100.00%

5000 4

I 129 257 312 29.20 29.40 29.60 29.80 n''’' 'I m/z SYTOO 48.84% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55

5000 ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ' ' I 29.20 29.40 29.60 29.80 m/z 43705 39790%

Tlfe-> 27

20 40 60 Abundance - -—— — 70

80 111125140 168 196 I' ' ' ' I T 100 120 140 160 180 200 220 240 260 280 300 #1354:1-Hexene; 2-methyl-— -- T I 5 JUA I I. . , I , “ , J 29.20 29.40 29.60 29.80 41 5000 m/z 41705 38774% 27

Ti/Z-> Abundance r 20 LU 40 60 98

80 100 120 140 160 180 200 220 240 260 280 300 r ''' I' ’'' I'''' I'''' I

.......... #44549; Butyl hexadecanoate--------- -------- ----- —5 ^ 29.20 29.40 29.60 ' 29.80 ~ ~ m/z 55.00 30750% ____ 5000 ___ 258

240 312 129 I ..,.157171185 214 '' ' I''''I'' ■' I''' ■ I''''I''' ' I''' I'''' I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

V23499.D NP091101.M Thu Oct 18 10:14:12 2001 Page 5

NYC-WtC_000088810

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NYC-WTC_000088810Source: NYC Law Department, mirrored locally

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