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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088811
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search-Gompound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Docosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.63 1.43 ug/1 172676 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual Docosane 310 C22H46 000629-97-0 93 2 Docosane, 9-butyl- 366 C26H54 055282-14-9 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 2678 (29.626 min): 23499.D (-) m/z 57700 100.00% 57

85 5000 4-

29.20 29.40 29.60 29.80 30.00 ■J , X jfM .................................. I?,'',? m/z 71.00 71.16% mfe-> 40 60 80 100 120 140 160 180 200 220 240*260 280 300 320 340 360 Abundance #72997: Docosane 3

71 5000 29.20 29.40 29.60 2980 30.00 “m/z 47700 70794% QQ " I' ' ' J J I I?® . 183 211 292 310 TTYTT*TT|T+TTp-rT*yrTM-|*TnnYrTYTp-rrTpTTTyTTTTpn-rryrTTTp-rTTpT-rrp-T-n m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance ” #73939: Docosane, 9-butyl- 57 I ' ' ' ' I V 29.20 29.40 29.60 29.80 30.00 5000 85 “mTz 87705 49794%

182 252 309 ggg ' I' I " H I H . 111 ri 11.1.1111.11111 I " '' I " " I " " I' " ' I " " I' " ' I" ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance——--------- -------------- —#71560: Octadecane — — 7- 29.20 29.40"29.60~29.80 30.00 m/z 41.00 30727%

5000 85

I 254 I r... I.. r. I.. I.. 111 I. I' " ' I " ‘' I " " I' " I TiZz-> 40 6080 100 120 140160180200 220240260 280 300320340 360 29.20 29.40 29.60 29.80 30.00

23499.D NP091101.M Thu Oct 18 10:14:15 2001 Page 6 NYC-WTC_000088811

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NYC-WTC_000088811Source: NYC Law Department, mirrored locally

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