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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088865
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091161.M (RTE.Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclobutane, 1,l-dimethyl-2-oc Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

29.50 3.76 ug/1 420892 Chrysene-dl2 33.12

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 Cyclob ane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 2 Cycl Xeptylamine 113 C7H15N 005452-35-7 27 3 1,3 /Hexanediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 4 0x1 rane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 25 fkbundance Scan 2665 (29.504 min): 23501 .D (-) m/z 56.00 100.00% 55

5000 41 73 129 257 . J 1^1571711^199213 [ 29.20 29.40 29.60 29.80 312 T. '“fl “1 « j T I ’ 1 j ' 'Tt I V I I . j ‘1 . I I I I 11 t j i' fl I yi I i' I I I 'I I t I I I Tj I T nH-ry m/z SYTOO 49704% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55

5000 /L a I' 1 f' I'' 29.20 29.40 29.60 29.80 mi/z 43.05 37.93% 27 70 Tt^tt I L 97 111125140 168 196 y-T-rVrYfT-iYyT-rfTyTT^^ I ‘ ‘ ' I I ' ' ' ' I ' '' ' I ' '' ‘ I' ' ' ' I''' ' I ■nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #2793: Cycloheplylamine 3

29.20 29.40 29.60 29.80 553 Tn/z 41705 37.62%

70 30 ■ ll I I ' ' ' ' I ' Tl/Z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 /Abundance #8882:1,3-Hexanediol, 2-ethyl- ' ‘ I ' ' 55 —29:20-29.40- 29.60- 29.80 - ' -m/z—73-. 00- 31.88%

5000 73 ft 31

■nZz-> I I ' ' ' ' I ' 20 40 ... I.-. 60 d 103 ....... 80 I' I'' I' I.. I 100 120 140 160 180 200 220 240 260 280 300 1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I . . ■ 29.20 29.40 29.60 29.80

23501.D NP091101.M Thu Oct 18 10:21:32 2001 Page 6

NYC-WTC_000088865

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NYC-WTC_000088865Source: NYC Law Department, mirrored locally

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