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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if******************** Peak Number 5 Cyclobutane, 1,1-dimethyl-2-oc Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.55 1.95 ug/1 268733 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolFoirm CAS# Qual

1 CycloMtane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 2 Butyyhexadecanoate 312 C2 0H40O2 000000-00-0 25 3 Oxir/ne, 2,3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 23 4 Nopane, 2,8-dimethyl-4-methylene- 168 C12H24 007323-15-1 16 Abundance Scan 2669 (29.545 min): 22582.D (-) Tm/z 56.00 100.00% 53

5000 4' I .oQ 257 ■p 101 239 29.20 29.40 29.60 29.80 -p-r-r-rp-r "r '''I'''' I'''' I m/z 57.00 49.60% TTfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1 -dimethyl-2-octyl- 53

5000- 29.20 29.40 29.60 29.80 m/z 41705 37.91% 27 ? I, 9,7 111125140 168 I p-rVryihrT-lYi-rWj^rTT-^^ 196 p-m-p-rr-ry I ' ' ' ' I ' ' ' ’ I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance

lUx #44549: Butyl hexadecanoate 53

29,20 29.40 29.60 29.80 5000 258 m/z 41.00 34.41% 240 312 129 I Il I 157171'*^ 214 pm-r-j- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- ' I'' •' I'' ' I 5 29.20 29.40 29,60 29.80 41 m/z 54.95 29.79%

5000

73

nfe-> 20 40 60 4, I 113128 ' ' I ‘ ■ I ‘ ' I 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29 60 29.80

22582.D NP091101.M Wed Oct 03 12:09:07 2001 Page 5

NYC-WTC_000d87262 '

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