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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087263
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ******************** *.* *********************************************** Peak Number 6 Pentacosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.74 0.60 ug/1 82051 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 2 Tricosane 324 C23H48 000638-67-5 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Octadecane ___________________ 254 C18H38 000593-45-3 90 Abundance Scan 2799 (30.739 min); 22582.D (-) m/z 57.00 100.00% 5j7 71 43 85 5000

30.40 30.60 30.80 31.00 , j|, .1. ....... ...... m/z 71.00 78.92% n/z-> Abundance 40 60

43 5,7 80 100 120 140 160 180 200 220 240 260 280 300 320 #73718: Pentacosane I 71 5000 r, I ,*. , T I n , , |*n“, I . I* 85 30.40 30.60 30.80 31.00 Wz 43.05 67.38% j I I ^II^I^^U1155169183197211225 r I I, IT. I ,■) 1,, I,I.I,,,, I..., 1111,1,,, 11 I '''' I ''' ‘ I ■nZz-> 40 60 80 100 ,120 140 160 180 200 220 240 260 280 300 320 ^bundance 43 5/

71 #73318: Tricosane L 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 50.72%

183197211225 296 324 l“’'' I ''''I'' " I' I'''' I'' '' I' ' ’ ' I'' ' p-rrTYT-TTT-yT^-T-ry-rTTTp-i-, Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193; Heptadecane 5/ 30,40 30,60 30.80 31.00 “m/z 41705 27.21% 71 5000 85

99 I 1^127141155169 210 240 I '' ' ' I ' ' r' I ■ , ' I f' ' • , I , ' ' ' I pn-TT^T-r-r-rl-r-rrT-f- I'' ‘ ' I ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

22582.D NP091101.M Wed Oct 03 12:09:09 2001 Page 6

NYC-WTC_000087263

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NYC-WTC_000087263Source: NYC Law Department, mirrored locally

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