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GC/MS analysis results for sample AD22582, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecanoic acid, 2-methylpro Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.68 1.52 ug/1 208581 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual (1jOctadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 84 ^"■'Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 72 3 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 4 1-Hexene, 2-methyl-98 C7H14 006094-02-6 35 Abundance Scan 2901 (31.675 min): 22582.D (-) m/z 56.00 100.00% Sb

5000 4' 73 285 ' ' I ' ' 1 I , or T 157 , 207 241 267 j 340 31.40 31.60 31.80 32.00 pr'if" m/z SYTOO 52.07% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5|7

5000 31.40 31.60 31.80 32.00 285 m7z 43.05 38.36% 7 97 129 267 J I II .1 ill I TT*Tp‘YT^iYrTY+p-ih-rj- 241 [ I “I I « I I I .Tn I I I I I i' I I I I I I I I I I 11 I 340 I”"f ■nfe-> 20 40 60 80 100.120 140 160 180 200 220 240 260 280 300 320 340 Sundance #40186; Butyl tetradecanoate (myristate) 5b 31.40 31.60 31.80 32.00 5000 m/z 41.00 36.37% 229 J •--73 211 129 284 I''" I' I . n . I .... I .... I I‘ 'I ' J " ' I' " ' I' " ' I ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 5b 31.40 31.60 31.80 32.00 m/z 55.00 29.01%

5000

27 I I 111:, , 111 140 168 11111111111111111 196 r''' 1 T ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22582.D NP091101.M Wed Oct 03 12:09:11 2001 Page 7

NYC-WTC_000087264

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NYC-WTC_000087264Source: NYC Law Department, mirrored locally

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