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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088842
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Octadecanoic acid, 2-methylpro Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.65 3.12 ug/1 314084 Chrysene-dl2 33.12 it# of 5 Tentative ID MW MolForm CAS# Qual

lyoctadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 87 z Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 64 3 Octadecanoic acid, butyl ester 340 C22H44O2. 000123-95-5 37 4 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 . 062338-30-1 27 Abundance Scan 2898 (31.647 min): 23500.D (-) m/z 56.00 100.00% 53

5000 4 73 129 285 340 31.40 31.60 31.80 32.00 ill p II 1 n r jV fI I j I 1 1 j I t ‘i I I I I I I j I J I I I I I I I j I I I I I 17 I I I r I I I I I I m/z 57.00 54.58% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester c: 7

5000 31.40 31.60 31.80 32.00 285 in/z 43.05 42.45% 7 97... 129 267 J I I, ,i I 241 I I 340 ''' ur*'' r I. I 111 I'''' I' ’'' I''' ‘ r ' ‘' I'''' I' u T Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 \bundance __ #40186: Butyl tetradecanoate (myristate) ---- 5fe- J \ ' 'T '31.40 31.60 31.80 32.00 5000 m/z 41.05 35.25% 229

I 7 211 284

nZz-> JUmXr 4^ I " " I • • > 11 " " I' r. . I.... I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Xbundance #73570: Octadecanoic acid, butyl ester 5b 31.40 31.60 31.80,32.00 m/z 73.00 33.72%

5000 ___ 285. 340 73 267 129 185 241 -nYrrT " I' ‘ " I'''' I'''' I " '' I'''' I' I '' ‘ '7 ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23500.D NP091101.M Thu Oct 18 10:18:01 2001 Page 10

NYC-WTC_000088842

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NYC-WTC_000088842Source: NYC Law Department, mirrored locally

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