Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Octadecanoic acid, 2-methylpro Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.68 1.56 ug/1 252715 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual (lyOctadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 84 2 Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 64 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 59 4 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance Scan 2901 (31.676 min): LBE.D (-) m/z 56.00 100.00% 53
5000 4- 73 129 285 . ....... 340 31.40 31.60 31.80 32.00 TT-p-I-TrfTT m/z SYTOO 52.82% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57
5000 31.40 31.60 31.80 32.00 285 m/z 43.05 41.27% 7*^ 267 J TT^rp^VTYYrTVfyrT’-rrjTTTT^^ ................ 340 fl n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 5)6 . T-| .-r, f'p-i I 31.40 31.60 31.80 32.00 5000 m/z 41.05 34.86% 229
L 73
L " ^29 .gg 211 284 I yy.Lj . I\ j-rm-r r ''' I ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 1' ' ' ' 1 ' ' ' ’ 1 53 31.40 31.60 31,80 32.00 m/z 55.00 32.06%
5000
Tl/Z-> 40 60 129 185 I I " '' I " '' I I ' ' ' ' I 241 r ' ' ' I 267
80 100 120 140 160 180 200 220 240 260 280 300 320 340 285 340
k 31.40 31.60 31.80 32.00
LBE.D NPO91101.M Wed Oct 03 14:41:18 2001 Page 11
NYC-WTC_000087148
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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