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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086778
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALOJ Sample : 9/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Octadecanoic acid, 2-methylpro Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.68 1.38 ug/1 312759 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolFoirm CAS# Qual I 1/Octadecanoic acid, 2-methylpropyl e 340 C22H44O2! 000646-13-9 87 Butyl tetradecanoate (myristate) 284 C18H36O2! 000000-00-0 72 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 50 4 Cyclobutane, 1,2-diethyl-, trans- 112 C8H16 019341-98-1 27 'Kbundance Scan 2902 (31.679 min): LBA.D (-) m/z 56700 100.00% 53 (1 5000 4 73 129 285

MU j, , 1.. 340 m/z 31.40 31.60 31.80 32,00 57.00 53751% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 31.40 31.60 31.80 32.00 285 m/z 43.05 39770% 267 J .1J i“i IV111r J1. 111 340 rrbn 241 I I I I ' I • I I I > • 11 ' I > I I ■ I . [ 1111 I Fl 111 Ti/k-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Naundance #40186; Butyl tetradecanoate (myristate) 53

_3t40_3t6p_^1J0_JZ00__ 5000 m/z 41.05 34.04% 229 , ” 129 211 284

tVz-> nU I ''' ' I''' ' I ' ' ' ' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570; Octadecanoic acid, butyl ester 53 31.40 31.60 31.80 32.00 m/z 73.00 29.45%

5000 285 340

a 73 267 129

ti/z-> 40 60 185 I I'''' I" ‘' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 xXL I ? 1*1 1 . t*| 1 1 I T“('Y7Ti"j TiT r 31.40 31.60 31.80 32.00

LBA.D NP091101.M Tue Oct 02 12:02:44 2001 Page 5

NYC-WTC_000086778

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