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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086777
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acg On : 1 Oct 2001 2:41 pm Operator: 209 GALOJ Sample ; 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K,L ********************************************************************** Peak Number 4 Heneicosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 30.73 0.52 ug/1 117588 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Tricosane 324 C23H48 000638-67-5 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 Abundance Scan 2799 (30.733 min): LBA.D (-) m/z 57.00 100.00% 43 71

5000 85

y.4O 30.60 30.80 31.00 ' I''' ' I'' '' I' ''' I'''' I ‘' m/z 71.10 77710% ttZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 5|7 71 85 5000 30.40 30,60 30.80 31.00 99 m/z43.0569791% ■ J, ■ A ■ ,V. ■ . ...... I................... I???.,, ......... nZz-> ' 60 80 ' 'lOo' w' 'l4o' 'l6o' 'iSO '200' '^0 240 2^ '280 3^ Abundance #73318: Tricosane 43 57 ' '’“1 *■ ' r'ppr I * 'Pr- 7 71 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 47.14%

183197211225 296 324 ■' 11'' ■' I'' TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71560: Octadecane \ 43 57 30.40 30.60 30.80 31.00 m/z 41.05 25.91% 71 85

99 lie

Ti/z-> Hr 169183197 1' 254 I''' ‘ I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 I 30.40 30.60 30.80 31.00

LBA.D NP091101.M Tue Oct 02 12:02:42 2001 Page 4

NYC-WTC_000086777

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NYC-WTC_000086777Source: NYC Law Department, mirrored locally

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