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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086776
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBA. D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 209 GALOS Sample 9/14 Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *************************************************** * * ************'^*** Peak Number 3 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 29.54 1.72 ug/1 390437 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexadecanoate 312 C20H40O2i 000000-00-0 38 2 Oxirany, 2,3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 32 3 1,3- xanediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 4 Cycl propane, 1-(1-methylethyl)-2-n 210 C15H30 041977-39-3 25 Abundance/ Scan 2669 (29.540 min): LBA.D (-) m/z 56.00 100.00% 53

5000 43 73 129 257 T T 29.20 29.40 29.60 29.80 312 • p • ' •1 • H, I m/z 57700 46.75% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 i\bundance #44549: Butyl hexadecanoate 55

itiXil 258 29.20 29.40 29,60 29.80 73 240 312 m/z 43.00 37.15% 116129 214 I y.N, 1^1/1 T I'''' I I'' ‘ ■ 1 T 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 53 41 29.20 29.40 29.60 29.80 553 m/z 41.05 37774% 73 113128 I''' 11' '' I''' ' I'''' I' '' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #66452:1,3-Hexanediol, 2-ethyl- T*-rr»-rrT^ I ' ' ' ' I 53 29.20 29.40 29.60 29.80 m/z 73.00 30.28% 5000- 73 103 31 J™, ........... ................ -........... .................. ................ .................... ' ' I ' ' ' ' I ' ' ' ' I ' ' ' '1 ' ' ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

LBA.D NP091101.M Tue Oct 02 12:02:40 2001 Page 3

NYC-WTC_00’0086776

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NYC-WTC_000086776Source: NYC Law Department, mirrored locally

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