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Document / 18 pages

GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086775
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 209 GALOf Sample 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params-. LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L *********************************************************************** Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.65 0.54 ug/1 105741 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 / Tentative ID MW MolForm CAS# Qual 1 1,4-DicM.orobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzen^l, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 2-Met^l-6-nitroaniline 152 C7H8N2O2i 000570-24-1 10 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 fthundance Scan 720 (11.648 min); LBA.D (-) m/z 149.90 100.00% 1!1O

5000 115 52 78 T 38 11.40 11.60 11.80 12.00 ‘ ‘ ‘ I' 4 4^ m/z 151.90 . 57.88% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichloroben2ene-d4 1!l0

5000 115 78 11.40 11.60 11.80 12.00 52 m7z'T^T790 34.63% 35 TTy-TT J.,......-..-. 4^ nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichioro- lilO T 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 77795 17732%

35 87 I T-p-rr-rp- I I • I ‘ ‘ I'''' I'''' I' ' mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883:2-Methyl-6-nitroaniline 77 1il2 11.40 11.60 11.80 12.00 m/z 52.00 . 14.18%

5000 106 52 94 ... I ' I n I . |l I '' I ' '' ' I ' ' 122 ' I'''' 11''' I' 41111111 T ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

LBA.D NP091101.M Tue Oct 02 12:02:38 2001 Page 2

NYC-WTC_000086775

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NYC-WTC_000086775Source: NYC Law Department, mirrored locally

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